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Quick method for separating target compounds from the bark of Maqian (Zanthoxylum myriacanthum var. pubescens) by high-performance countercurrent chromatography
Qingfei Fan; Huanli Zhang; Huabin Hu; Youkai Xu; Qishi Song
2016
Source PublicationJOURNAL OF SEPARATION SCIENCE
Volume39Issue:20Pages:4049-4052
AbstractChoosing a suitable solvent system for a countercurrent chromatography separation presents a challenge for many researchers. In this study, we introduce a quick method of separating a target compound from the bark of Zanthoxylum myriacanthum var. pubescens by countercurrent chromatography. This method relies on the thin-layer chromatography based generally useful estimation of solvent systems. This paper will present how to quickly choose a suitable solvent system with a thin-layer chromatography based generally useful estimation of solvent systems working chart. O-Methyltembamide (1) was enriched by countercurrent chromatography using n-hexane/ethyl acetate/methanol/water (6:4:6:4) as the solvent system. Further purification was achieved by high-performance liquid chromatography with purities of 98.2% from Z. myriacanthum var. pubescens bark.
Document Type期刊论文
Identifierhttp://ir.xtbg.org.cn/handle/353005/10102
Collection民族植物学研究组
Recommended Citation
GB/T 7714
Qingfei Fan,Huanli Zhang,Huabin Hu,et al. Quick method for separating target compounds from the bark of Maqian (Zanthoxylum myriacanthum var. pubescens) by high-performance countercurrent chromatography[J]. JOURNAL OF SEPARATION SCIENCE,2016,39(20):4049-4052.
APA Qingfei Fan,Huanli Zhang,Huabin Hu,Youkai Xu,&Qishi Song.(2016).Quick method for separating target compounds from the bark of Maqian (Zanthoxylum myriacanthum var. pubescens) by high-performance countercurrent chromatography.JOURNAL OF SEPARATION SCIENCE,39(20),4049-4052.
MLA Qingfei Fan,et al."Quick method for separating target compounds from the bark of Maqian (Zanthoxylum myriacanthum var. pubescens) by high-performance countercurrent chromatography".JOURNAL OF SEPARATION SCIENCE 39.20(2016):4049-4052.
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